HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58413253, compound → HCID 58413331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58413253 | HCID 58413253 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58413331 | HCID 58413331 | — |
Reaction Steps
3-Nitro-2-(1,1,1-trifluoropropan-2-yloxy)pyridine (6.2 g) was dissolved in methanol (500 ml) and Raney nickel (1.0 g) was added. The reaction mixture was hydrogenated at room temperature and 5 bar. The catalyst was filtered off and the filtrate was concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853193B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-99be2db461544b39b71a033ba3746a0d |
| Source note | uspto-grants-2014_10 |