Dimethylformamide dimethyl acetal → HCID 68941755, compound

HRID 532425Notes

Reaction equation

HRID 532425 reaction equation
[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH2:13][CH2:14][C:15]([OH:18])([CH3:17])[CH3:16])=[CH:8][C:9]=1[N+:10]([O-])=O)=[O:4].CO[CH:21]([N:24]([CH3:26])[CH3:25])OC>>[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH2:13][CH2:14][C:15]([OH:18])([CH3:17])[CH3:16])=[CH:8][C:9]=1[N:10]=[CH:21][N:24]([CH3:26])[CH3:25])=[O:4]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 68936540HCID 68936540, compound

Product 1

HCID 68941755HCID 68941755, compound

Procedure

5-(3-Hydroxy-3-methylbutyl)-3-nitrothiophene-2-carboxylic acid methyl ester was reacted with dimethoxymethyldimethylamine by method B. The product with the molecular weight of 298.41 (C14H22N2O3S) was obtained in this way; MS (ESI): 299.1 (M+H+).

Workup

  1. customThe product with the molecular weight of 298.41 (C14H22N2O3S) was obtained in this way

Sources & evidence

ORD record
ord-7c8038993ad94062b93c28e50d427627
Source dataset
uspto-grants-2014_10
Patent number
US08853208B2

Reaction notes

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