HCID 68944112, compound → HCID 68943596, compound

Participants

Reaction Steps

A suspension of 8-Methyl-3-(2-methyl-4-nitro-phenoxy)-8-aza-bicyclo[3.2.1]octane (495 mg) and palladium (5% on carbon; 63 mg) in methanol (25 mL) was stirred vigorously under a hydrogen atmosphere (atmospheric pressure) for 2 h. Then the catalyst was filtered off and the filtrate concentrated. The product with the molecular weight of 246.35 (C15H22N20); was obtained in this way; MS (ESI) 247 (M+H+).

Provenance & Evidence