Dimethylformamide dimethyl acetal → HCID 57618681, compound

HRID 532446Notes

Reaction equation

HRID 532446 reaction equation
[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH2:11][O:12][Si:13]([C:26]([CH3:29])([CH3:28])[CH3:27])([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:8][C:9]=1[NH2:10])=[O:4].CO[CH:32]([N:35]([CH3:37])[CH3:36])OC>>[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH2:11][O:12][Si:13]([C:26]([CH3:29])([CH3:28])[CH3:27])([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:8][C:9]=1[N:10]=[CH:32][N:35]([CH3:37])[CH3:36])=[O:4]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 68943581HCID 68943581, compound

Product 1

HCID 57618681HCID 57618681, compound

Procedure

3-Amino-5-(tert-butyldiphenylsilanyloxymethyl)thiophene-2-carboxylic acid methyl ester and dimethoxymethyldimethylamine were reacted by method B. The product with the molecular weight of 480.71 (C26H32N2O3SSi) was obtained in this way; MS (ESI): 481 (M+H+).

Workup

  1. customThe product with the molecular weight of 480.71 (C26H32N2O3SSi) was obtained in this way

Sources & evidence

ORD record
ord-b50781460c7543c6b9e15ace3c47beb1
Source dataset
uspto-grants-2014_10
Patent number
US08853208B2

Reaction notes

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