Potassium Carbonate → HCID 68941697, compound
Reaction equation
[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([C:17]2([OH:23])[CH2:22][CH2:21][O:20][CH2:19][CH2:18]2)=[CH:8][C:9]=1[NH:10]C(=O)C(F)(F)F)=[O:4].C(=O)([O-])[O-].[K+].[K+]>>[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([C:17]2([OH:23])[CH2:18][CH2:19][O:20][CH2:21][CH2:22]2)=[CH:8][C:9]=1[NH2:10])=[O:4]Participants
3
Procedure
5-(4-Hydroxytetrahydropyran-4-yl)-3-(2,2,2-trifluoroacetylanino)thiophene-2-carboxylic acid methyl ester and potassium carbonate were reacted by method GA. The product with the molecular weight of 257.31 (C11H15NO4S) was obtained in this way; MS (ESI): 258 (M+H+).
Workup
- customThe product with the molecular weight of 257.31 (C11H15NO4S) was obtained in this way
Sources & evidence
- ORD record
- ord-9f4ffbcac04642f4820993e13a6e5f7c
- Source dataset
- uspto-grants-2014_10
- Patent number
- US08853208B2
Reaction notes
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