Trifluoroacetic acid → HCID 178511732, compound

Participants

Reaction Steps

tert-Butyl N-[(3S,5R)-2-(2,5-difluorophenyl)-5-(4,6-dihydro-2H-pyrrolo[3,4-c]pyrazol-5-yl)tetrahydrothiopyran-3-yl]carbamate (3.2 mg, 0.007 mmol) was dissolved in a mixture of TFA (0.5 mL) and methylene chloride (1.0 mL) and stirred at RT for 1 h. The solvents were evaporated and the residue was freeze-dried from a mixture of benzene and ethanol to give the title compound as a white solid.

Provenance & Evidence