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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 532532Generated: October 31, 2026

Trifluoroacetic acid → HCID 178511733, compound

https://huagongshe.com/reaction/532532

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 178454096HCID 178454096—
SolventDichloromethaneHCID 6344—
ProductHCID 178511733HCID 178511733—

Reaction Steps

tert-Butyl N-[(3S,5R)-5-(4,6-dihydro-2H-pyrrolo[3,4-c]pyrazol-5-yl)-1-oxo-2-(2,3,5-trifluorophenyl)thian-3-yl]carbamate was dissolved in a mixture of TFA (0.02 mL) and methylene chloride (0.2 mL). After stirring at RT for 105 min, the solvents were evaporated and the residue was freeze-dried from a mixture of benzene and ethanol to give the title compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08853212B2
Source datasetuspto-grants-2014_10
ORD IDord-5d28f72bba65432194f70ad86be09161
Source noteuspto-grants-2014_10