HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178511733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178454096 | HCID 178454096 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178511733 | HCID 178511733 | — |
Reaction Steps
tert-Butyl N-[(3S,5R)-5-(4,6-dihydro-2H-pyrrolo[3,4-c]pyrazol-5-yl)-1-oxo-2-(2,3,5-trifluorophenyl)thian-3-yl]carbamate was dissolved in a mixture of TFA (0.02 mL) and methylene chloride (0.2 mL). After stirring at RT for 105 min, the solvents were evaporated and the residue was freeze-dried from a mixture of benzene and ethanol to give the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853212B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-5d28f72bba65432194f70ad86be09161 |
| Source note | uspto-grants-2014_10 |