HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 533137Generated: October 29, 2026
HCID 86667501, compound → HCID 86667500, compound
https://huagongshe.com/reaction/533137
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 86667501 | HCID 86667501 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 86667500 | HCID 86667500 | 85.7% |
Reaction Steps
A mixture of 2-chloro-6-methoxy-nicotinic acid hydrochloride salt (360 g, 1925 mmol) in thionyl chloride (500 mL) was stirred at 80° C. for 5 h. The solvent was evaporated in vacuo to yield 2-chloro-6-methoxy-nicotinoyl chloride (340 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08853237B2 |
|---|
| Source dataset | uspto-grants-2014_10 |
|---|
| ORD ID | ord-2a8c33d8af8944d999a0bd277821af44 |
|---|
| Source note | uspto-grants-2014_10 |
|---|
