反应详情

A mixture of ethyl-2-indole carboxylate (1.89 g) and N-bromosuccinimide (1.77 g) in THF (30 mL) was stirred at room temperature for 1 hour. The mixture was poured into water (150 mL) and filtered. The filtrate was washed with THF, dried under vacuum at 60° C., and recrystallized from ethyl acetate/hexanes.

1. filtrationfiltered
2. washThe filtrate was washed with THF
3. customdried under vacuum at 60° C.
4. customrecrystallized from ethyl acetate/hexanes