HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic acid dihydrate → HCID 86731815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic acid dihydrate | HCID 61373 | — |
| Reactant | Lurasidone | HCID 213046 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86731815 | HCID 86731815 | — |
Reaction Steps
A mixture consisting of isopropanol (600 mL), lurasidone base (57 g) and oxalic acid dihydrate (15 g) is refluxed for about an hour, and then cooled for two hours at ambient temperature. The solid is filtered, and 62 g of substantially pure lurasidone oxalate is obtained after drying.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853395B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-87b6eb023cf247239b05cbd8559e0ad6 |
| Source note | uspto-grants-2014_10 |