Tetrahydrofuran → HCID 66795818, compound

Participants

Reaction Steps

Following the general procedure, reaction of 6b (3.70 g assayed, 12.0 mmol) with 1 M BH3 in THF (42.0 mL, 42.0 mmol) afforded 7b in an assay yield of 2.77 g (9.4 mmol, 78% assay yield, 99% peak area). A sample was concentrated in vacuo to an oil to provide the standard.

Provenance & Evidence