Tetrahydrofuran → HCID 66795803, compound

Participants

Reaction Steps

Following the general procedure, reaction of 6c (3.55 g assayed, 12.0 mmol) with 1 M BH3 in THF (42.0 mL, 42.0 mmol) afforded 7c in an assay yield of 2.98 g (10.6 mmol, 88% assay yield, 99% peak area). A sample was concentrated in vacuo to an oil to provide the standard.

Provenance & Evidence