Tetrahydrofuran → HCID 66796247, compound

Participants

Reaction Steps

Following the general procedure, reaction of 6d (3.22 g assayed, 12.0 mmol) with 1 M BH3 in THF (42.0 mL, 42.0 mmol) afforded 7d in an assayed yield of 2.21 g (8.7 mmol, 73% assay yield, 99% peak area). A sample was concentrated in vacuo to an oil to provide the standard.

Provenance & Evidence