HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 66796176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 66796076 | HCID 66796076 | — |
| Product | HCID 66796176 | HCID 66796176 | — |
Reaction Steps
Following the general procedure, reaction of 6e (4.20 g assayed, 13.55 mmol) with 1 M BH3 in THF (47.4 mL, 47.4 mmol) afforded 7e in an assay yield of 2.68 g (9.05 mmol, 67% assay yield, 100% peak area). A sample was concentrated in vacuo to an oil to provide the standard.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853390B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-34d7b277b7fe4029a922ca6a2d1d8c0a |
| Source note | uspto-grants-2014_10 |