Tetrahydrofuran → HCID 66796274, compound

Participants

Reaction Steps

Following the general procedure, reaction of 6f (3.95 g assayed, 13.42 mmol) with 1 M BH3 in THF (40.3 mL, 40.3 mmol) afforded 7f in an assay yield of 3.15 g (11.25 mmol, 84% assay yield, 100% peak area). A sample was concentrated in vacuo to an oil to provide the standard.

Provenance & Evidence