HuagongsheHuagongshe Chemistry Print Report · For research reference only
3(2H)-Pyridazinone → HCID 66796051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3(2H)-Pyridazinone | HCID 68153 | — |
| Reactant | HCID 66795818 | HCID 66795818 | — |
| Product | HCID 66796051 | HCID 66796051 | — |
Reaction Steps
Following the general procedure, reaction of 7b (2.67 g assayed, 9.08 mmol) with 3(2H)-pyridazinone (1.14 g, 11.8 mmol) afforded a solution of the free base of 8b in an assayed yield of 2.61 g (93% assay yield, 95% peak area).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853390B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-693cccdb90a8489b994962b0e19ee625 |
| Source note | uspto-grants-2014_10 |