HuagongsheHuagongshe Chemistry Print Report · For research reference only
3(2H)-Pyridazinone → HCID 66796057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3(2H)-Pyridazinone | HCID 68153 | — |
| Reactant | HCID 66795803 | HCID 66795803 | — |
| Product | HCID 66796057 | HCID 66796057 | — |
Reaction Steps
Following the general procedure, reaction of 7c (2.87 g assayed, 10.2 mmol) with 3(2H)-pyridazinone (1.27 g, 13.2 mmol) afforded a solution of the free base of 8c in an assayed yield of 2.55 g (84% assay yield, 93% peak area).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853390B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-250c22adbd4f43d489ede88cd902747b |
| Source note | uspto-grants-2014_10 |