HuagongsheHuagongshe Chemistry Print Report · For research reference only
3(2H)-Pyridazinone → HCID 66795884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3(2H)-Pyridazinone | HCID 68153 | — |
| Reactant | HCID 66796247 | HCID 66796247 | — |
| Product | HCID 66795884 | HCID 66795884 | — |
Reaction Steps
Following the general procedure, reaction of 7d (2.13 g assayed, 8.37 mmol) with 3(2H)-pyridazinone (1.05 g, 10.5 mmol) afforded a solution of the free base of 8d in an assayed yield of 1.57 g (5.8 mmol, 70% assay yield, 93% peak area).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853390B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-b66ab8c4c6884d43872087eea135d712 |
| Source note | uspto-grants-2014_10 |