HuagongsheHuagongshe Chemistry Print Report · For research reference only
3(2H)-Pyridazinone → HCID 66795981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3(2H)-Pyridazinone | HCID 68153 | — |
| Reactant | HCID 66796176 | HCID 66796176 | — |
| Product | HCID 66795981 | HCID 66795981 | — |
Reaction Steps
Following the general procedure, reaction of 7e (2.59 g assayed, 8.75 mmol) with 3(2H)-pyridazinone (1.09 g, 11.37 mmol) afforded a solution of the free base of 8e in an assayed yield of 2.03 g (50% assay yield, 96% peak area).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853390B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-dec1b2e1482a41139bb50385632ca5af |
| Source note | uspto-grants-2014_10 |