HRID5339

反应详情

EQUATION

反应方程式

HRID 5339 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

26.8 g of 4-bromophenol was taken under protective gas in 1000 ml of dioxane, mixed with 90 g 3-tributylstannylpyridine [preparation according to litt.: Org. Magn. Resonance, 7 (1975), 610] and 11.1 g of bis-(triphenylphosphine)-palladium(II) chloride and refluxed for 15 hours. After concentration by evaporation in a vacuum and purification on silica gel, 15.92 g of the above compound is isolated.

WORKUP

后处理

  1. temperaturerefluxed for 15 hours
  2. concentrationAfter concentration
  3. customby evaporation
  4. customin a vacuum and purification on silica gel