HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86715098, compound → HCID 86715097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86715098 | HCID 86715098 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 86715097 | HCID 86715097 | — |
Reaction Steps
A mixture of (R)-3-(4-benzyloxy-phenoxy)-pyrrolidin-2-one (61 g), MeOH/DCM (2:1, 2 L) and Pd (10% on carbon, 6 g) was shaken under an atmosphere of hydrogen for 20 hours. The catalyst was removed by filtration and the filtrate concentrated to provide the subtitle compound. MS ESI+: m/z=194 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853412B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-61079ac8544c4126bbe85a195a2c927d |
| Source note | uspto-grants-2014_10 |