HCID 86715106, compound → HCID 136377298, compound

Participants

Reaction Steps

A solution of methyl 2-(5-(4-methoxybenzyloxy)pyridin-2-yl)thiazole-5-carboxylate (1.10 g) in TFA (10 mL) was stirred at 80° C. for 2 hours. After the reaction was complete, the mixture was evaporated. The residue was purified by silica gel column chromatography eluting with ethyl acetate/petroleum ether (1:2 to pure EA) to provide the subtitle compound. MS ESI+: m/z=237 [M+H]+.

Provenance & Evidence