huagongshe.com
HRID534725

反应详情

EQUATION

反应方程式

HRID 534725 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccc([N+](=O)[O-])cc1
HCID541

4-Nitrobenzaldehyde

C7H5NO3

结构：CC(C)(C)OC(=O)N1CCNCC1
HCID143452

tert-Butyl piperazine-1-carboxylate

C9H18N2O2

结构：C[C@H]1CN(Cc2ccc([N+](=O)[O-])cc2)CCN1C(=O)OC(C)(C)C
HCID59262204

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCN(Cc2ccc([N+](=O)[O-])cc2)CC1
HCID23506946

tert-Butyl 4-[(4-nitrophenyl)methyl]piperazine-1-carboxylate

C16H23N3O4

PROCEDURE

实验过程

The title compound was prepared from 4-nitrobenzaldehyde and 1,1-dimethylethyl 1-piperazinecarboxylate using a method similar to that described for D1 in Description 1A although the product was purified by column chromatography followed by passing through an SCX column eluting with MeOH then 2M NH3 in MeOH. MS (ES+): 266.1, 222.2, no molecular ion (MH+) observed.

WORKUP

后处理

  1. customwas purified by column chromatography
  2. washeluting with MeOH