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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 534773Generated: October 30, 2026

tert-Butyl methylcarbamate → 1,1-Dimethylethyl (4-formyl-3-methylphenyl)methylcarbamate

https://huagongshe.com/reaction/534773

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttert-Butyl methylcarbamateHCID 527635—
Reactant4-Bromo-2-methylbenzaldehydeHCID 13555150—
Product1,1-Dimethylethyl (4-formyl-3-methylphenyl)methylcarbamateHCID 86618112—

Reaction Steps

The title compound was prepared from crude 4-bromo-2-methylbenzaldehyde (D91) and 1,1-dimethylethyl methylcarbamate (D83) using a method similar to that described for D84 in Description 84. δH (CDCl3, 400 MHz) 10.20 (1H, s), 7.76 (1H, d), 7.28 (1H, dd), 7.19 (1H, d), 3.31 (3H, s), 2.66 (3H, s), 1.49 (9H, s).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08853218B2
Source datasetuspto-grants-2014_10
ORD IDord-a4151cb120db4f1fb6a9f1696b683330
Source noteuspto-grants-2014_10