Caprolactam → HCID 131731937, compound

HRID 535216Notes

Reaction equation

HRID 535216 reaction equation
[C:1]1(=[O:8])[NH:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[S-:9][C:10]#[N:11].[NH4+:12]>>[C:1]1(=[O:8])[NH:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[S-:9][C:10]#[N:11].[NH4+:12]

Participants

3

Reactant 2

HCID 7768CaprolactamHCID 15666Ammonium thiocyanate

Product 1

HCID 131731937HCID 131731937, compoundYield 219.2%

Conditions

Temperature
50 °C

Procedure

To a round-bottom flask, 8.92 g of purified caprolactam and 2 g of NH4SCN (ammonium thiocyanate) were introduced. The mixture was agitated gradually under nitrogen atmosphere at 50° C. for 4 hours and cooled to room temperature to obtain 10.9 g of caprolactam-NH4SCN eutectic mixture.

Workup

  1. temperaturecooled to room temperature

Sources & evidence

ORD record
ord-6200493794a74ccab36624d2874f9177
Source dataset
uspto-grants-2014_10
Patent number
US08858837B2

Reaction notes

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