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HRID535286

反应详情

EQUATION

反应方程式

HRID 535286 的结构方程式

REACTANTS

反应物

2
结构：O=C1CCC(=O)O1
HCID7922

Succinic anhydride

C4H4O3

结构：CC(C)(C)OC(=O)NCCOCCOCCN
HCID9881394

tert-Butyl {2-[2-(2-aminoethoxy)ethoxy]ethyl}carbamate

C11H24N2O4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCOCCOCCNC(=O)CCC(=O)O
HCID57325707

未命名化合物

收率 98%

PROCEDURE

实验过程

Preparation from 1-(t-butyloxycarbonylamino)-3,6-dioxa-8-octanamine) (5 g, 20.16 mmol) and succinic anhydride (2.218 g, 22.18 mmol) gave a thick yellow oil which crystallised on standing (6.5 g, yield 98%). LCMS (Method 6): Rt 2.99 min; m/z (M+1) 349; Calcd.: 349.

WORKUP

后处理

  1. customgave a thick yellow oil which
  2. customcrystallised