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HRID535288

反应详情

EQUATION

反应方程式

HRID 535288 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCCOCCOCCNC(=O)CCC(=O)O
HCID57325707

未命名化合物

结构：CC(C)(C)OC(=O)CCCCCCC(=O)ON1C(=O)CCC1=O
HCID59760896

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)CCCCCCC(=O)NCCOCCOCCNC(=O)CCC(=O)O
HCID59476999

未命名化合物

收率 132.2%

PROCEDURE

实验过程

Octanedioic acid tert-butyl ester 2,5-dioxo-pyrrolidin-1-yl ester (1.13 g, 3.45 mmol) and N-{2-[2-(2-tert-butoxycarbonylamino-ethoxy)-ethoxy]-ethyl}-succinamic acid (1 g, 2.874 mmol) were reacted as described above. 1.75 g crude product was isolated and used without further purification. LCMS (Method 6): Rt 3.86 min; m/z (M+1) 461; Calcd.: 461.