4-Chlorophenylacetyl chloride → HCID 71469053, compound

Participants

Reaction Steps

The product of Example 4B was treated with 2-(4-chlorophenyl)acetyl chloride similar to the method described in Example 4C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.76 (s, 1H), 8.65 (dd, J=2.5, 0.8 Hz, 1H), 8.39-8.43 (m, 1H), 8.13 (dd, J=8.2, 2.5 Hz, 1H), 7.86-8.02 (m, 2H), 7.67-7.81 (m, 2H), 7.37-7.44 (m, 4H), 3.71 (s, 2H); MS (ESI+) M/Z 425 (M+H)+.

Provenance & Evidence