HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorophenylacetic acid → HCID 70976097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Reactant | HCID 70976322 | HCID 70976322 | — |
| Product | HCID 70976097 | HCID 70976097 | — |
Reaction Steps
The product from Example 14B and 2-(3,5-difluorophenyl)acetic acid was processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.78 (s, 1H), 8.39-8.42 (m, 1H), 7.90-8.05 (m, 2H), 7.73 (d, J=5.1 Hz, 1H), 7.62-7.65 (m, 1H), 7.08-7.22 (m, 4H), 3.77 (s, 2H), 2.10 (s, 3H); MS (APCI) M/Z 412 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-a1d22093d68144b0a5296772e384124f |
| Source note | uspto-grants-2014_10 |