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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 535494Generated: October 30, 2026

3,5-Difluorophenylacetic acid → HCID 70976254, compound

https://huagongshe.com/reaction/535494

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 21262530HCID 21262530—
ProductHCID 70976254HCID 70976254—

Reaction Steps

The product from Example 18A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ 11.83 (s, 1H), 8.78 (ddd, J=4.8, 1.7, 0.9, 1H), 8.46-8.30 (m, 2H), 7.99 (dddd, J=16.4, 15.3, 7.5, 1.6, 3H), 7.80 (dt, J=7.8, 1.0, 1H), 7.59 (ddd, J=7.6, 4.8, 1.1, 1H), 7.23-7.09 (m, 3H), 3.79 (s, 2H); MS (APCI) M/Z 393 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08859549B2
Source datasetuspto-grants-2014_10
ORD IDord-3fc2b0908d574559b0e194865539ee2c
Source noteuspto-grants-2014_10