4-Chlorophenylacetyl chloride → HCID 70976126, compound

Participants

Reaction Steps

The product from Example 57B and 2-(4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ 11.69 (s, 1H), 8.34 (dd, J=7.9, 1.1, 1H), 8.08 (d, J=7.4, 1H), 8.00 (td, J=7.7, 1.5, 1H), 7.94 (td, J=7.6, 1.3, 1H), 7.40 (d, J=8.8, 9H), 3.66 (s, 2H); MS (APCI+) M/Z 422 (M+H)+.

Provenance & Evidence