3,5-Difluorophenylacetic acid → HCID 70975778, compound

Participants

Reaction Steps

The product from Example 60A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.54-11.55 (m, 1H), 8.30-8.34 (m, 1H), 8.01-8.04 (m, 1H), 7.96-8.01 (m, 1H), 7.87-7.92 (m, 1H), 7.11-7.19 (m, 3H), 3.84-3.93 (m, 2H), 3.73 (s, 2H), 3.32-3.36 (buried m, 2H), 2.40-2.47 (m, 2H), 1.12 (d, J=6.2 Hz, 6H); MS (APCI+) M/Z 429 (M+H)+.

Provenance & Evidence