3,5-Difluorophenylacetic acid → HCID 56927667, compound

Participants

Reaction Steps

The product from Example 68B and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (500 MHz, CDCl3) δ ppm 8.69-8.72 (m, 1H), 8.44-8.47 (m, 1H), 8.31-8.35 (bs, 1H), 8.00-8.06 (m, 2H), 7.93-7.98 (m, 1H), 7.85-7.90 (m, 1H), 7.66-7.70 (m, 1H), 7.55-7.61 (m, 2H), 6.82-6.91 (m, 2H), 6.74-6.81 (m, 1H), 3.69-3.74 (bs, 2H); MS (APCI+) M/Z 456 (M+H)+.

Provenance & Evidence