4-Chlorophenylacetyl chloride → HCID 70673582, compound

Participants

Reaction Steps

The product from Example 68B and (4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (500 MHz, CDCl3) δ ppm 8.67-8.69 (m, 1H), 8.43 (d, J=8.0 Hz, 1H), 8.22-8.24 (bs, 1H), 8.00-8.04 (m, 2H), 7.90-7.97 (m, 1H), 7.82-7.87 (m, 1H), 7.66-7.70 (m, 1H), 7.54-7.58 (m, 2H), 7.33-7.36 (m, 2H), 7.24-7.30 (m, 2H), 3.71-3.74 (bs, 2H); MS (APCI+) M/Z 454 (M+H)+.

Provenance & Evidence