4-Chlorophenylacetyl chloride → HCID 70976138, compound

Participants

Reaction Steps

The product from Example 76B and 2-(4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.80-11.82 (bs, 1H), 8.96-8.99 (m, 1H), 8.40-8.46 (m, 1H), 8.12 (s, 1H), 7.96-8.04 (m, 3H), 7.71-7.79 (m, 1H), 7.36-7.44 (m, 4H), 3.72 (s, 2H); MS (APCI) M/Z 459 (M+H)+.

Provenance & Evidence