Methanesulfonyl chloride → HCID 70975849, compound

Participants

Reaction Steps

The product from Example 42 and methanesulfonyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.66-11.72 (m, 1H), 8.31-8.43 (m, 1H), 8.15 (d, J=8.0 Hz, 1H), 7.99-8.06 (m, 1H), 7.89-7.96 (m, 1H), 7.66-7.74 (bs, 1H), 7.36-7.45 (m, 4H), 4.46-4.49 (m, 2H), 3.68 (s, 2H), 2.94 (s, 3H); MS (ESI+) M/Z 421 (M+H)+.

Provenance & Evidence