Phenylacetyl chloride → HCID 70975741, compound

Participants

Reaction Steps

The product from Example 42 and 2-phenylacetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (500 MHz, CDCl3) δ ppm 8.42 (d, J=7.8 Hz, 1H), 8.11-8.13 (bs, 1H), 7.83-7.91 (m, 2H), 7.76-7.82 (m, 1H), 7.39 (s, 3H), 7.23-7.35 (buried m, 6H), 6.24-6.30 (bs, 1H), 4.72-4.74 (m, 2H), 3.79-3.80 (bs, 2H), 3.63-3.63 (bs, 2H); MS (ESI−) M/Z 459 (M−H)−.

Provenance & Evidence