HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorophenylacetic acid → HCID 70975864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Reactant | HCID 70976237 | HCID 70976237 | — |
| Product | HCID 70975864 | HCID 70975864 | — |
Reaction Steps
The product from Example 91B and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.55 (s, 1H), 8.30 (d, J=7.9 Hz, 1H), 7.84-8.02 (m, 3H), 7.05-7.19 (m, 3H), 3.73 (s, 2H), 2.83-2.87 (m, 4H); MS (APCI+) M/Z 417 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-01c202afa9744a3a8a215d5f31eab724 |
| Source note | uspto-grants-2014_10 |