4-Chlorophenylacetyl chloride → HCID 131731941, compound

Participants

Reaction Steps

The product from Example 103B and 2-(4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ 10.83-10.76 (m, 1H), 8.30-8.25 (m, 1H), 8.06-7.99 (m, 1H), 7.99-7.93 (m, 1H), 7.93-7.86 (m, 1H), 7.44 (d, J=8.8, 2H), 7.41-7.37 (m, 2H), 7.35-7.31 (m, 4H), 3.53 (s, 2H), 1.32 (s, 9H); MS (APCI+) M/Z 537 (M+H)+.

Provenance & Evidence