1-Methylpiperazine → HCID 70975947, compound
Reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5](=[O:12])[NH:4][N:3]=1.[CH3:13][N:14]1[CH2:19][CH2:18][NH:17][CH2:16][CH2:15]1>>[CH3:13][N:14]1[CH2:19][CH2:18][N:17]([C:2]2[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5](=[O:12])[NH:4][N:3]=2)[CH2:16][CH2:15]1Participants
3
Procedure
4-chlorophthalazin-1-one and 1-methylpiperazine were treated using methods similar to that described in Examples 1A to give the title compound. MS (APCI+) M/Z 245 (M+H)+.
Sources & evidence
- ORD record
- ord-43f2f31f2885422cae724cb04e06b135
- Source dataset
- uspto-grants-2014_10
- Patent number
- US08859549B2
Reaction notes
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