4-Chlorophenylacetyl chloride → HCID 70976342, compound

Participants

Reaction Steps

The product from Example 107B and (4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ 11.55 (s, 1H), 9.77 (s, 1H), 8.32 (d, J=7.9, 1H), 8.03-7.97 (m, 2H), 7.96-7.89 (m, 1H), 7.45-7.36 (m, 4H), 3.68 (s, 2H), 3.65-3.50 (m, 4H), 3.08-2.98 (m, 2H), 2.91 (s, 3H), 2.49-2.44 (buried m, 2H); MS (APCI+) M/Z 412 (M+H)+.

Provenance & Evidence