4-Chlorophenylacetyl chloride → HCID 70975846, compound

Participants

Reaction Steps

The product of Example 109B and 2-(4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ 11.60 (s, 1H), 8.34 (d, J=7.8, 1H), 8.05-7.96 (m, 2H), 7.92 (ddd, J=8.1, 6.1, 2.3, 1H), 7.45-7.35 (m, 4H), 4.52 (q, J=7.1, 1H), 4.12-3.99 (m, 2H), 3.68 (s, 2H), 1.46 (d, 3H), 1.06 (t, 3H); MS (ESI+) M/Z 414 (M+H)+.

Provenance & Evidence