3,3,3-Trifluoropropionic acid → HCID 70976207, compound

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Reaction Steps

The product of Example 1B and 3,3,3-trifluoropropanoic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.32 (dd, J=7.9, 1.3 Hz, 1H), 8.04 (dd, J=8.1, 1.3 Hz, 1H), 7.98-8.02 (m, 1H), 7.93 (td, J=7.5, 1.3 Hz, 1H), 3.82-3.84 (m, 4H), 3.53-3.60 (m, 2H), 3.09-3.11 (m, 4H); MS (ESI+) M/Z 357 (M+H)+.

Provenance & Evidence