HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Nitrophenyl)acetic acid → HCID 70975844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Nitrophenyl)acetic acid | HCID 77337 | — |
| Reactant | 2-amino-4-morpholinophthalazin-1(2H)-one | HCID 70976104 | — |
| Product | HCID 70975844 | HCID 70975844 | — |
Reaction Steps
The product of Example 1B and 2-(2-nitrophenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/D2O) δ 8.30 (d, J=7.7, 1H), 8.09-7.95 (m, 4H), 7.94-7.87 (m, 1H), 7.73 (dt, J=7.6, 3.8, 1H), 7.63 (d, J=6.7, 1H), 7.59 (dd, J=11.2, 4.4, 1H), 4.13 (s, 2H), 3.86-3.79 (m, 4H), 3.14-3.04 (m, 4H); MS (ESI+) M/Z 410 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-6e7077df109049be9933d762685f95c4 |
| Source note | uspto-grants-2014_10 |