Hydroxyphenylacetic acid → HCID 70975891, compound

Participants

Reaction Steps

The product of Example 1B and 2-(4-hydroxyphenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.30 (dd, J=7.9, 1.2 Hz, 1H), 8.03 (d, J=8.0 Hz, 1H), 7.97-8.00 (m, 1H), 7.89-7.92 (m, 1H), 7.18 (s, 2H), 6.75 (d, 2H), 3.81-3.83 (m, 4H), 3.53 (s, 2H), 3.07-3.11 (m, 4H); MS (ESI−) M/Z 379 (M−H)−.

Provenance & Evidence