(3-Methoxyphenyl)acetic acid → HCID 70976130, compound

Participants

Reaction Steps

The product of Example 1B and 2-(3-methoxyphenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.31 (dd, J=7.9, 1.3 Hz, 1H), 7.97-8.05 (m, 2H), 7.91 (td, J=7.5, 1.3 Hz, 1H), 7.27 (t, J=7.8 Hz, 1H), 6.98-6.99 (m, 1H), 6.96 (d, J=7.6 Hz, 1H), 6.86 (dd, J=8.2, 2.6 Hz, 1H), 3.81-3.83 (m, 4H), 3.77 (s, 3H), 3.63 (s, 2H), 3.03-3.13 (m, 4H); MS (ESI−) M/Z 393 (M−H)−.

Provenance & Evidence