(3-Bromophenyl)acetic acid → HCID 70976170, compound

Participants

Reaction Steps

The product of Example 1B and 2-(3-bromophenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.31 (dd, J=7.9, 1.3 Hz, 1H), 8.04 (d, J=8.0 Hz, 1H), 7.97-8.01 (m, 1H), 7.89-7.93 (m, 1H), 7.60 (t, J=1.8 Hz, 1H), 7.49 (dt, J=7.8, 1.5 Hz, 1H), 7.39 (d, J=7.6 Hz, 1H), 7.34 (t, J=7.7 Hz, 1H), 3.83 (d, J=4.2 Hz, 4H), 3.69 (s, 2H), 3.09-3.11 (m, 4H); MS (ESI−) M/Z 441 (M−H)−.

Provenance & Evidence