Benzeneacetic acid, 4-bromo- → HCID 70976173, compound

Participants

Reaction Steps

The product of Example 1B and 2-(4-bromophenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.30 (dd, J=7.9, 1.3 Hz, 1H), 8.03 (dd, J=8.1, 1.3 Hz, 1H), 7.97-8.01 (m, 1H), 7.91 (td, J=7.5, 1.3 Hz, 1H), 7.54-7.56 (m, 2H), 7.33-7.36 (m, 2H), 3.78-3.83 (m, 4H), 3.65 (s, 2H), 3.08-3.13 (m, 4H); MS (ESI−) M/Z 441 (M−H)−.

Provenance & Evidence