HuagongsheHuagongshe Chemistry Print Report · For research reference only
Felbinac → HCID 70976129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Felbinac | HCID 3332 | — |
| Reactant | 2-amino-4-morpholinophthalazin-1(2H)-one | HCID 70976104 | — |
| Product | HCID 70976129 | HCID 70976129 | — |
Reaction Steps
The product of Example 1B and 2-(biphenyl-4-yl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.32 (d, J=7.9 Hz, 1H), 8.04 (d, J=8.0 Hz, 1H), 7.97-8.01 (m, 1H), 7.89-7.93 (m, 1H), 7.56-7.69 (m, 4H), 7.47-7.50 (m, 4H), 7.38 (t, J=7.4 Hz, 1H), 3.78-3.84 (m, 4H), 3.72 (s, 2H), 3.09-3.11 (m, 4H); MS (ESI+) M/Z 441 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-fd825b326c304fd49984b88bfa8ea6b8 |
| Source note | uspto-grants-2014_10 |