3,4-Dichlorophenylacetic acid → HCID 70975877, compound

Participants

Reaction Steps

The product of Example 1B and 2-(3,4-dichlorophenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.31 (dd, J=7.9, 1.3 Hz, 1H), 8.03 (d, J=8.0 Hz, 1H), 7.97-8.01 (m, 1H), 7.89-7.93 (m, 1H), 7.66 (d, J=2.0 Hz, 1H), 7.63 (d, J=8.2 Hz, 1H), 7.37 (dd, J=8.2, 2.1 Hz, 1H), 3.80-3.84 (m, 4H), 3.72 (s, 2H), 3.08-3.11 (m, 4H); MS (ESI−) M/Z 431 (M−H)−.

Provenance & Evidence